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Author Topic: Reaction CX-7 (Experimental)  (Read 815 times)

Basquyatti

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Reaction CX-7 (Experimental)
« on: September 15, 2018, 02:27:43 am »
My experimental synthesis to obtain Halogenated oximes.

Summary: This reaction uses a cheaper process of reducing Chloropicrin with the help of Magnesium and
anhydrous hydrogen chloride in a closed container, the standard solvent is Tetrahydrofuran, the reaction takes place at low temperatures and on vigorous shaking as soon as all the material is precipitated at the bottom, water is added to precipitate insoluble, then these are filtered, the solvent distilled and the CX purified by vacuum distillation.

Using 167.72 grams of PS 99%, place to mix with 600 grams of 99% THF at 0 degrees Celsius and place the mixture in a pressure-holding vessel, then introduce 49,102 grams of 99% Magnesium powder, and close the container with vigorously stir, pour into it 109.5 grams of anhydrous Hydrogen Chloride, the reaction ends when there is no more pressure in the vessel, then it filters the impurities, distills the solvent from 66 degrees Celsius up to 70 degrees Celsius and distils the agent at 58 degrees Celsius by 28 mmHg
« Last Edit: September 15, 2018, 03:13:43 am by Basquyatti »

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zwclose7

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Re: Reaction CX-7 (Experimental)
« Reply #1 on: October 01, 2018, 12:42:28 am »
Are you Basquyatti from Wikipedia?

Basquyatti

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Re: Reaction CX-7 (Experimental)
« Reply #2 on: October 02, 2018, 12:12:33 am »
Yes, I am the Basquyati of the Portuguese Wikipedia

zwclose7

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Re: Reaction CX-7 (Experimental)
« Reply #3 on: October 02, 2018, 12:46:47 am »
Are you a chemist?

 

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